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Titel A new device to mount portable energy dispersive X-ray fluorescence spectrometers (p-ED-XRF) for semi-continuous analyses of split (sediment) cores and solid samples
VerfasserIn Philipp Hoelzmann, Torsten Klein, Frank Kutz, Brigitta Schütt
Konferenz EGU General Assembly 2016
Medientyp Artikel
Sprache en
Digitales Dokument PDF
Erschienen In: GRA - Volume 18 (2016)
Datensatznummer 250124749
Publikation (Nr.) Volltext-Dokument vorhandenEGU/EGU2016-4234.pdf
 
Zusammenfassung
Portable energy-dispersive X-ray fluorescence spectrometers (p-ED-XRF) have become increasingly popular in sedimentary laboratories to quantify the chemical composition of a range of materials such as sediments, solid samples, and artefacts. Here, we introduce a low-cost, clearly arranged unit that functions as a sample chamber (German industrial property right no. 20 2014 106 048.0) for p-ED-XRF devices to facilitate economic, non-destructive, fast, and semi-continuous analysis of (sediment) cores and/or other solid samples. The spatial resolution of the measurements is limited to the specifications of the applied p-ED-XRF device – in our case a Thermo Scientific NITON XL3t p-ED-XRF spectrometer with a maximum spatial resolution of 1 cm and equipped with a charge-coupled device (CCD)-camera to document the measurement spot. We demonstrate the strength of combining p-ED-XRF analyses with this new sample chamber to identify Holocene facies changes (e.g. marine vs terrestrial sedimentary facies) using a sediment core from an estuarine environment in context of a geoarchaeological investigation at the Atlantic coast of southern Spain.