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Titel Experimental investigation of structures and rheology on halite single-crystals: In-situ approach.
VerfasserIn D. Picard, A. Dimanov, J. Raphanel
Konferenz EGU General Assembly 2012
Medientyp Artikel
Sprache Englisch
Digitales Dokument PDF
Erschienen In: GRA - Volume 14 (2012)
Datensatznummer 250060254
 
Zusammenfassung
Intracrystalline plasticity, coupled with the rheological properties, are key parameters to constrain the flow behavior of rock salt. Crystal plasticity is inherently anisotropic and therefore polycrystalline materials always exhibit heterogeneous behavior which results from local scale incompatibility and involves additional accommodation mechanisms (micro-cracking, grain sliding-€¦). It is thus important to understand the interaction between neighboring grains and inside single crystals. For this reason, we investigate crystal plasticity of halite single-crystals (NaCl) with compression experiments performed inside a scanning electron microscope (SEM). Starting materials consist of high purity halite single crystals of approximately 5x5x10mm. Micro droplets of gold are deposited on the polished sample surface in order to provide very fine markers for the Digital Image Correlation (DIC) technique used to evaluate the surface displacement field at several steps of the loading process. The DIC method allows to compute the strain field and to evaluate quantitatively the heterogeneity of the local deformation which can be related to local mechanisms such as intracrystalline slip. Compression experiments were performed along {001} using an uniaxial press installed inside a SEM. Tests were performed at room temperature, a strain rate 9.4x10-5 s-1  5%. Moreover, from one step to another, the deformation accommodated by a slip band can vary from 1% to 10%. These preliminary results indicate that, even with simple loading tests and easy slip systems, important heterogeneity of deformation occurs. Further experiments at higher temperature and with different loading orientation will also be presented.